demonstrations:gravity_filtration
Gravity Filtration
Materials: ★★☆ Available in most school laboratories or specialist stores
Difficulty: ★☆☆ Can be easily done by most teenagers
Safety: ★☆☆ Minimal safety procedures required
Categories: Lab Skills and Safety
Alternative titles:
Summary
Gravity filtration is a laboratory method used to separate a solid residue from a liquid filtrate by passing the mixture through filter paper held in a funnel. The technique allows suspended solids to be collected while the clear liquid passes through.
Procedure
- Set up a ring stand with a ring clamp and place a funnel over a receiving flask. Use a clay triangle if needed to support the funnel.
- Position the flask so its neck touches the funnel tip to reduce splashing.
- Insert filter paper into the funnel. Use fluted filter paper by unfolding it so the folds touch the funnel, or prepare a flat disc by folding it twice with a slight angle and tearing a small corner to help it fit smoothly.
- Wet the filter paper with deionized water so it adheres to the funnel walls.
- Pour the liquid mixture down a glass rod into the funnel, ensuring the rod touches the funnel wall to prevent splashing. Keep the funnel filled to about two-thirds.
- Continue pouring before the funnel empties, rinsing any residue from the glass rod into the funnel.
- Transfer any remaining solid with a rubber policeman or a wash bottle to ensure complete collection.
- Rinse the solid on the filter paper with small amounts of water, letting it drain between washes.
- Once filtration is complete, carefully remove the filter paper. The solid left behind is the residue, while the clear liquid collected is the filtrate.
Links
Demonstration of Filtration - Rugby School Chemistry:
📄 Filtration by Gravity - Valencia College: https://science.valenciacollege.edu/chemistry/techniques/tech16-filtrationgravity.pdf
Variations
- Use vacuum (Büchner) filtration for faster separation when fine particles or large volumes are involved.
- Test different types of filter paper (fluted, plain, or pre-weighed) depending on the experiment’s requirements.
Safety Precautions
- Wear safety goggles and a lab coat to protect from splashes.
- Handle glassware carefully to avoid breakage and cuts.
- Use caution with the wash bottle to prevent over-spraying liquids.
- Dispose of residue and filtrate according to laboratory waste guidelines.
Questions to Consider
- Why is it important to wet the filter paper before filtering? (It seals the paper against the funnel, preventing solids from bypassing the filter.)
- What is the difference between residue and filtrate? (Residue is the solid left on the filter paper; filtrate is the liquid that passes through.)
- Why should the tip of the glass rod touch the funnel wall while pouring? (It prevents splashing and loss of material.)
- How does fluted filter paper improve the filtration process? (It increases surface area and allows liquid to pass more quickly.)