======Sublimation of Iodine====== **Materials: **{{$demo.materials_description}}\\ **Difficulty: **{{$demo.difficulty_description}}\\ **Safety: **{{$demo.safety_description}}\\ \\ **Categories:** {{$demo.categories}} \\ **Alternative titles:** Solid to Vapor Transition of Iodine ====Summary==== {{$demo.summary}} ====Procedure==== - Place about 2 g of iodine crystals into a 500 ml Erlenmeyer flask. - Cover the mouth of the flask with a watch glass that has ice placed on top. - Slowly heat the flask on a hot plate. - Observe as purple iodine vapor forms and deposits solid iodine crystals on the underside of the watch glass. ====Links==== Chemistry experiment 47 - Sublimation of Iodine - koen2all: {{youtube>jX9pskbKSw0?}}\\ 📄 The Sublimation of Iodine - lsa.umich: [[https://lsa.umich.edu/content/dam/chem-assets/chem-docs/teaching%20lab%20docs/Sublimation%20of%20Iodine.pdf]]\\ ====Variations==== * Use a test tube instead of a flask for a smaller-scale demonstration. * Capture time-lapse images to show the sublimation and deposition process. * Compare sublimation with substances that melt before vaporizing, highlighting differences in phase changes. ====Safety Precautions==== * Wear safety goggles, gloves, and a lab coat. * Iodine vapors are toxic and irritating; perform the demonstration in a fume hood. * Avoid skin contact with iodine crystals. * Dispose of iodine-containing waste according to hazardous chemical waste guidelines. ====Questions to Consider==== * What type of phase change does iodine undergo in this experiment? (Sublimation, solid to gas.) * Why do iodine crystals form on the cooled watch glass? (The vapor condenses and deposits as solid iodine upon cooling.) * How does sublimation differ from melting and boiling? (Sublimation skips the liquid phase, going directly from solid to gas.) * Can you name other substances that undergo sublimation under standard conditions? (Dry ice, naphthalene.)