======Gravity Filtration====== **Materials: **{{$demo.materials_description}}\\ **Difficulty: **{{$demo.difficulty_description}}\\ **Safety: **{{$demo.safety_description}}\\ \\ **Categories:** {{$demo.categories}} \\ **Alternative titles:** ====Summary==== {{$demo.summary}} ====Procedure==== - Set up a ring stand with a ring clamp and place a funnel over a receiving flask. Use a clay triangle if needed to support the funnel. - Position the flask so its neck touches the funnel tip to reduce splashing. - Insert filter paper into the funnel. Use fluted filter paper by unfolding it so the folds touch the funnel, or prepare a flat disc by folding it twice with a slight angle and tearing a small corner to help it fit smoothly. - Wet the filter paper with deionized water so it adheres to the funnel walls. - Pour the liquid mixture down a glass rod into the funnel, ensuring the rod touches the funnel wall to prevent splashing. Keep the funnel filled to about two-thirds. - Continue pouring before the funnel empties, rinsing any residue from the glass rod into the funnel. - Transfer any remaining solid with a rubber policeman or a wash bottle to ensure complete collection. - Rinse the solid on the filter paper with small amounts of water, letting it drain between washes. - Once filtration is complete, carefully remove the filter paper. The solid left behind is the residue, while the clear liquid collected is the filtrate. ====Links==== Demonstration of Filtration - Rugby School Chemistry: {{youtube>cQT9U-EJU4o?}}\\ 📄 Filtration by Gravity - Valencia College: [[https://science.valenciacollege.edu/chemistry/techniques/tech16-filtrationgravity.pdf]]\\ ====Variations==== * Use vacuum (Büchner) filtration for faster separation when fine particles or large volumes are involved. * Test different types of filter paper (fluted, plain, or pre-weighed) depending on the experiment’s requirements. ====Safety Precautions==== * Wear safety goggles and a lab coat to protect from splashes. * Handle glassware carefully to avoid breakage and cuts. * Use caution with the wash bottle to prevent over-spraying liquids. * Dispose of residue and filtrate according to laboratory waste guidelines. ====Questions to Consider==== * Why is it important to wet the filter paper before filtering? (It seals the paper against the funnel, preventing solids from bypassing the filter.) * What is the difference between residue and filtrate? (Residue is the solid left on the filter paper; filtrate is the liquid that passes through.) * Why should the tip of the glass rod touch the funnel wall while pouring? (It prevents splashing and loss of material.) * How does fluted filter paper improve the filtration process? (It increases surface area and allows liquid to pass more quickly.)