======Angle of Repose====== **Materials: **{{$demo.materials_description}}\\ **Difficulty: **{{$demo.difficulty_description}}\\ **Safety: **{{$demo.safety_description}}\\ \\ **Categories:** {{$demo.categories}} \\ **Alternative titles:** Determining the Flow Properties of Powders ====Summary==== {{$demo.summary}} ====Procedure==== - Prepare several samples of sand with different particle sizes or mixtures. - Place each sample in a cylinder or container with a removable base. - Lift the cylinder vertically, allowing the sand to flow freely and form a heap on a flat surface. - Measure the height and base diameter of the heap using a ruler. - Calculate the angle of repose using the formula: θ = tan⁻¹(height / radius) - Repeat the process for each sand type, including one with added moisture or glidant. - Record all measurements and compare the calculated angles to assess flow properties. ====Links==== Angle of Repose | Determination of Angle of Repose With Calculation | Angle of Repose - Solution- Pharmacy: {{youtube>lPYz4iNfwzw?}}\\ ANGLE OF REPOSE | HOW TO PERFORM IN LABORATORY? DETAIL CALCULATION | IMPORTANCE OF FLOW PROPERTY - PHARMAROCKS THE WAY OF SUCCESS: {{youtube>rPCOUitcOV4?}}\\ 📄 Angle of Repose - Pharmaceutical Technology: [[https://pharmatechno2014.blogspot.com/p/d-angle-of-repose.html]]\\ ====Variations==== * Repeat the experiment using different powders. * Compare dry and slightly damp samples to examine the effect of moisture. * Use mechanical methods such as a tilting box or revolving cylinder to measure dynamic angles of repose. ====Safety Precautions==== * Work on a clean, stable surface to prevent spills or contamination. * Handle glassware and measuring tools carefully. ====Questions to Consider==== * Which sand sample had the lowest angle of repose, and what does that indicate? (A lower angle indicates better flowability.) * How does particle size affect flow characteristics? (Smaller particles increase cohesion, leading to higher angles of repose.) * What is the effect of adding moisture or glidant? (Moisture increases cohesion and the angle of repose, while glidants reduce it.) * How does particle shape influence the results? (Round particles roll more easily and form lower angles than irregular ones.) * What alternative methods can be used to measure angle of repose? (Tilting box, fixed funnel, or revolving cylinder methods.)